돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1461808생성일: 2026년 10월 25일

Dimethylamine → 1-Butanone, 2-(dimethylamino)-1-(4-(dimethylamino)phenyl)-2-(phenylmethyl)-

https://huagongshe.com/reaction/1461808

반응식

참여 물질

역할이름HCID투입량
반응물DimethylamineHCID 674—
반응물Potassium CarbonateHCID 11430—
반응물2-Benzyl-2-(dimethylamino)-1-(4-fluorophenyl)butan-1-oneHCID 19360599—
용매DimethylformamideHCID 6228—
생성물1-Butanone, 2-(dimethylamino)-1-(4-(dimethylamino)phenyl)-2-(phenylmethyl)-HCID 164106—

반응 단계

A stirred autoclave is filled with 50 g (0.167 mol) of 1-(4-fluorophenyl)-2-dimethylamino-2-benzylbutan-1-one (crude product from B), 300 ml of dimethylformamide and 23.1 g (0.167 mol) of potassium carbonate. 22.6 g (0.5 mol) of dimethylamine are then added under pressure (3-4 bar). The mixture is heated to 100° and stirred at this temperature for 24 hours.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05077402
출처 데이터셋uspto-grants-1991_12
ORD IDord-8e07e5cda52743a79a7241d5b9115f72
출처 메모uspto-grants-1991_12