Glyoxal → HCID 15099950, compound

HRID 1461884Notes

Reaction equation

HRID 1461884 reaction equation
[CH2:1]([PH2:4])[CH2:2][CH3:3].[CH:5]([CH:7]=[O:8])=[O:6]>O1CCCC1>[CH2:1]([P:4]1[CH:5]([OH:6])[CH:7]([OH:8])[P:4]([CH2:1][CH2:2][CH3:3])[CH:5]([OH:6])[CH:7]1[OH:8])[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 7860GlyoxalHCID 14647240Propylphosphane

Product 1

HCID 15099950HCID 15099950, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Following the procedure of Example 1, mono-n-propylphosphine, in tetrahydrofuran, as solvent, is reacted with a 40% aqueous glyoxal solution, to give 1,4-di-n-propyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a solid melting at 131°-133° C.

Sources & evidence

ORD record
ord-fc956f540c7d47db95ca7ad18a631d56
Source dataset
uspto-grants-1991_12
Patent number
US05077437

Reaction notes

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