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HRID1461899

反应详情

EQUATION

反应方程式

HRID 1461899 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1cccc([N+](=O)[O-])c1
HCID7452

1,3-Dinitrobenzene

C6H4N2O4

结构：C[O-].[Na+]
HCID10942334

Methanol, sodium salt

CH3NaO

PRODUCTS

生成物

1
结构：COc1cccc([N+](=O)[O-])c1
HCID11140

Benzene, 1-methoxy-3-nitro-

C7H7NO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)P(=O)(N(C)C)N(C)C
溶剂HCID12679

Hexamethylphosphoramide

C6H18N3OP

PROCEDURE

实验过程

m-Nitroanisole was prepared by reacting m-dinitrobenzene with sodium methoxide at 25° C. for 16 hours in hexamethylphosphotriamide solvent (N. Kornblum et al., J. Org. Chem., 41, 1560 (1976)).

WORKUP

后处理

  1. customat 25° C.
  2. customfor 16 hours