HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorobenzoyl isocyanate → Teflubenzuron
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorobenzoyl isocyanate | HCID 2733369 | — |
| Reactant | 3,5-Dichloro-2,4-difluorobenzenamine | HCID 2774000 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Teflubenzuron | HCID 91734 | — |
Reaction Steps
Three grams (0.016 mol) of 2,6-difluoro-benzoyl isocyanate were added to a solution of 2.95 gm (0.015 mol) of 2,4-difluoro-3,5-dichloroaniline in 50 ml of toluene. The solution thus obtained was stirred for 15 hours at room temperature. Thereafter, the product which precipitated during that time was removed by suction filtration and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04457943 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-9bf4f69978b74406ae77f12ebb41fc96 |
| Source note | uspto-grants-1984_07 |