HRID1462014

反应详情

EQUATION

反应方程式

HRID 1462014 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Three grams (0.016 mol) of 2,6-difluoro-benzoyl isocyanate were added to a solution of 2.95 gm (0.015 mol) of 2,4-difluoro-3,5-dichloroaniline in 50 ml of toluene. The solution thus obtained was stirred for 15 hours at room temperature. Thereafter, the product which precipitated during that time was removed by suction filtration and dried.

WORKUP

后处理

  1. customThe solution thus obtained
  2. customThereafter, the product which precipitated during that time
  3. customwas removed by suction filtration
  4. customdried