Diisopropylamine → 90477-06-8

HRID 1462027Notes

Reaction equation

HRID 1462027 reaction equation
[Cl:1][CH:2]([CH3:6])[C:3](Cl)=[O:4].[CH:7]([NH:10][CH:11]([CH3:13])[CH3:12])([CH3:9])[CH3:8]>CO>[CH:7]([N:10]([CH:11]([CH3:13])[CH3:12])[C:3](=[O:4])[CH:2]([Cl:1])[CH3:6])([CH3:9])[CH3:8]

Participants

4

Reactant 2

HCID 7912DiisopropylamineHCID 1110192-Chloropropionyl chloride

Product 1

HCID 1334509690477-06-8

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Reaction of 2-chloropropionylchloride with diisopropylamine under the experimental conditions of Example 16, gives the product; b.p. 87°-88° (0.1 mm); Rf=0.67 (methanol); IR (neat) νmax: 2960, 2920, 1650, 1475, 1450, 1370, 1340, 1210, 1040, 620 cm-1 ; Cl (Schoeninger) calculated %: 18.49--Found %: 18.43.

Workup

  1. customgives the product

Sources & evidence

ORD record
ord-22d4efd297e446f9a81244af66eb2238
Source dataset
uspto-grants-1984_07
Patent number
US04457931

Reaction notes

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