HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → 90477-06-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | 2-Chloropropionyl chloride | HCID 111019 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 90477-06-8 | HCID 13345096 | — |
Reaction Steps
Reaction of 2-chloropropionylchloride with diisopropylamine under the experimental conditions of Example 16, gives the product; b.p. 87°-88° (0.1 mm); Rf=0.67 (methanol); IR (neat) νmax: 2960, 2920, 1650, 1475, 1450, 1370, 1340, 1210, 1040, 620 cm-1 ; Cl (Schoeninger) calculated %: 18.49--Found %: 18.43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04457931 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-22d4efd297e446f9a81244af66eb2238 |
| Source note | uspto-grants-1984_07 |