HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 12882232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | HCID 12850342 | HCID 12850342 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12882232 | HCID 12882232 | 95% |
Reaction Steps
1.5 g of KCN and 1.8 ml of acetic acid were added to 2.5 g of the aldehyde thus obtained dissolved 40 ml of ethanol and then left overnight under stirring. Then, the reaction mixture was poured into 100 ml of 2N-HCl and the extraction was effected with benzene. After washing with NaCl aqueous solution, the benzene layer was condensed to yield 2.7 g of 3-anilino-α-cyanobenzylalcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04457940 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-398c759f12914f9ea691e45f87fc466e |
| Source note | uspto-grants-1984_07 |