HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Hydroxide → HCID 86739521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Reactant | HCID 86739519 | HCID 86739519 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86739521 | HCID 86739521 | — |
Reaction Steps
To a solution of 13.5 g of 4-hydroxy-3-nitrophenylmethylsulfone in 100 ml of ethanol are added 41 g of a 40% aqueous tetrabutylammonium hydroxide solution. The resultant deep yellow solution is evaporated in a rotovap to give 28 g of yellow crystal product with a melting point of 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04459152 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-7a0fe596c81b4d58bac5961b58e8c73b |
| Source note | uspto-grants-1984_07 |