Phenylhydrazine → HCID 13127487, compound

HRID 1462147Notes

Reaction equation

HRID 1462147 reaction equation
C1([NH:7]N)C=CC=CC=1.[Cl:9][C:10]1[CH:16]=[C:15]([CH2:17][CH3:18])[CH:14]=[C:13]([Cl:19])[C:11]=1[NH2:12]>>[Cl:9][C:10]1[CH:16]=[C:15]([CH2:17][CH3:18])[CH:14]=[C:13]([Cl:19])[C:11]=1[NH:12][NH2:7]

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 13127655HCID 13127655, compound

Product 1

HCID 13127487HCID 13127487, compound

Procedure

The phenylhydrazine used as starting material in Reference Example 10 was prepared by proceeding in a similar manner to that hereinbefore described in Reference Example 5 but replacing the 2-chloro-4-ethylaniline by 2,6-dichloro-4-ethylaniline. 2,6-Dichloro-4-ethylphenylhydrazine, m.p. 48°-50° C., was obtained in the form of a cream-coloured solid.

Workup

  1. customwas prepared

Sources & evidence

ORD record
ord-c5103b7744c642a988cc2f4b643473cd
Source dataset
uspto-grants-1984_07
Patent number
US04459150

Reaction notes

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