HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydantoin → HCID 20454111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydantoin | HCID 10006 | — |
| Reactant | 2H-1,2,4-Oxadiazin-3(4H)-one, dihydro-5-thioxo- | HCID 3006908 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20454111 | HCID 20454111 | 41% |
Reaction Steps
To a solution of 1.0 g (0.0075 mole) of 6H-1,2,4-oxadiazin-3(2H)-one-5(4H)-thione in 50 ml of freshly distilled dry dioxane is added 0.77 g (0.0077 mole) of hydantoin. After stirring at room temperature for 17 hours, the solution is filtered, washed with chloroform and dried to give a yield of 0.6 g (41 percent) of 1-(3,6-dihydro-3-oxo-2H-1,2,4-oxadiazin-5-yl)-2,4-imidazolidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04459403 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-98a0acb4a4e34e86a6817b12f43a520e |
| Source note | uspto-grants-1984_07 |