Allylamine → HCID 178437616, compound

HRID 1462223Notes

Reaction equation

HRID 1462223 reaction equation
[CH2:1]([NH2:4])[CH:2]=[CH2:3].[N:5](=[C:7]([C:11](=[O:13])[CH3:12])[C:8](=O)[CH3:9])O>C(#N)C>[C:11]([C:7]1[NH:5][C:1]([CH:2]=[CH2:3])=[N:4][C:8]=1[CH3:9])(=[O:13])[CH3:12]

Participants

4

Reactant 2

HCID 7853AllylamineHCID 178468373HCID 178468373, compound

Product 1

HCID 178437616HCID 178437616, compoundYield 76.8%

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

An acetonitrile solution of allylamine (0.4 g, 7.8 mmol) and 3-oximino-2,4-pentanedione (1 g, 7.8 mmol) was refluxed for 6 hours. The acetonitrile was evaporated to give 0.9 g of 5-acetyl-4-methyl-2-vinylimidazole.

Workup

  1. customThe acetonitrile was evaporated

Sources & evidence

ORD record
ord-d87452f01a3b46afa5fd1143d6ee9989
Source dataset
uspto-grants-1984_07
Patent number
US04459413

Reaction notes

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