HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13295055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 13295054 | HCID 13295054 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13295055 | HCID 13295055 | — |
Reaction Steps
2-(4-Aminophenoxy)-5-chloropyrimidine (20 g), was dissolved in acetic acid (100 ml), and acetic anhydride (20 ml) was added to the solution. After standing for a period of 5 minutes the solution was heated on a steam bath and hot water (100 ml) was slowly added. On cooling the product crystallised and was collected and dried. Yield 20 g, m.p. 202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460588 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-f263e038054c4b26a8bf1d9f778bbf0e |
| Source note | uspto-grants-1984_07 |