HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13105435, compound → HCID 23693741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13105435 | HCID 13105435 | — |
| Reactant | Potassium hydroxide methanol | HCID 23689386 | — |
| Product | HCID 23693741 | HCID 23693741 | 80% |
Reaction Steps
2.7 g of ethyl 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate are dissolved in 10 ml of 10% potassium hydroxide/methanol, and the solution is stirred at room temperature for 17 hours. After the reactioh, the crystalline precipitates are collected by filtration, and then washed with cold ethanol and ether. 2.4 g of potassium 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-893afefeceed4b6396854eac9e46d57d |
| Source note | uspto-grants-1984_07 |