HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 13105448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Oxazoleacetic acid, 2-(p-fluorophenyl)-5-(3-thienyl)- | HCID 3069787 | — |
| Product | HCID 13105448 | HCID 13105448 | 42.2% |
Reaction Steps
2 g of 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetic acid, 0.5 g of potassium hydroxide, 4.2 g of oxalyl chloride and 20 ml of n-butanol are treated in the same manner as described in Example 17. One g of n-butyl 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate is thereby obtained. Yield: 42.2%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-f51f1ce18588414bbab4aacce861f7db |
| Source note | uspto-grants-1984_07 |