HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → n-Butyl 2-[2-(4-chlorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | 2-Chloro-1-methylpyridinium iodide | HCID 167069 | — |
| Reactant | 2-[2-(4-Chlorophenyl)-5-(3-thienyl)-4-oxazolyl]acetic acid | HCID 13105440 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | n-Butyl 2-[2-(4-chlorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate | HCID 13105451 | 69.6% |
Reaction Steps
0.55 g of 2-[2-(4-chlorophenyl)-5-(3-thienyl)-4-oxazolyl]acetic acid, 0.44 g of 2-chloro-1-methyl-pyridinium iodide, 0.13 ml of n-butanol and 0.2 g of triethylamine are treated in the same manner as described in Example 20. 0.45 g of n-butyl 2-[2-(4-chlorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate is thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-e422d2ca544449b2b27b9a268a90f865 |
| Source note | uspto-grants-1984_07 |