HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-benzoyl-N-[(3-thienylcarbonyl)methyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(3-thienyl)ethanone hydrochloride | HCID 13105417 | — |
| Product | N-benzoyl-N-[(3-thienylcarbonyl)methyl]amine | HCID 13105427 | 95.1% |
Reaction Steps
4 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 8 g of sodium bicarbonate and 3.6 g of benzoyl chloride are treated in the same manner as described in Preparation 1-(3). 5.25 g of N-benzoyl-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-a84de10dd2d546fe8d3fcde273ed33d6 |
| Source note | uspto-grants-1984_07 |