HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → N-(4-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(3-thienyl)ethanone hydrochloride | HCID 13105417 | — |
| Product | N-(4-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine | HCID 13105428 | 94.9% |
Reaction Steps
19.4 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 36 g of sodium bicarbonate and 21 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 29 g of N-(4-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-2f48792d60c64a48b4cb978d87aa16f7 |
| Source note | uspto-grants-1984_07 |