HRID1462423

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8501

4-Chlorobenzoyl chloride

C7H4Cl2O

HCID516892

Sodium Bicarbonate

CHNaO3

HCID13105417

2-Amino-1-(thiophen-3-yl)ethan-1-one--hydrogen chloride (1/1)

C6H8ClNOS

PRODUCTS

生成物

HCID13105428

未命名化合物

收率 94.9%

PROCEDURE

实验过程

19.4 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 36 g of sodium bicarbonate and 21 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 29 g of N-(4-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.

WORKUP

后处理

customas described in Preparation 1-(3)