HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → N-(4-chlorobenzoyl)-N-[(2-thienylcarbonyl)methyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(thiophen-2-yl)ethan-1-one hydrochloride | HCID 12609833 | — |
| Product | N-(4-chlorobenzoyl)-N-[(2-thienylcarbonyl)methyl]amine | HCID 13105423 | 99.5% |
Reaction Steps
5.0 g of N-[(2-thienylcarbonyl)methyl]amine hydrochloride, 10.0 g of sodium bicarbonate and 4.78 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 7.6 g of N-(4-chlorobenzoyl)-N-[(2-thienylcarbonyl)methyl]amine are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-a2eb3f821adf42b497db155ae0a20373 |
| Source note | uspto-grants-1984_07 |