HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3-chloro- → N-(3-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(3-thienyl)ethanone hydrochloride | HCID 13105417 | — |
| Product | N-(3-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine | HCID 13105430 | 93.1% |
Reaction Steps
7.5 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 10.0 g of sodium bicarbonate and 8.86 g of 3-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 11.0 g of N-(3-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-38156cc5e28e49adb731aec2d3476634 |
| Source note | uspto-grants-1984_07 |