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HRID1462431

反应详情

EQUATION

反应方程式

HRID 1462431 的结构方程式

REACTANTS

反应物

3
结构：O=C(Cl)c1cccc(Cl)c1
HCID69252

Benzoyl chloride, 3-chloro-

C7H4Cl2O

结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：Cl.NCC(=O)c1ccsc1
HCID13105417

2-Amino-1-(thiophen-3-yl)ethan-1-one--hydrogen chloride (1/1)

C6H8ClNOS

PRODUCTS

生成物

1
结构：O=C(CNC(=O)c1cccc(Cl)c1)c1ccsc1
HCID13105430

未命名化合物

收率 93.1%

PROCEDURE

实验过程

7.5 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 10.0 g of sodium bicarbonate and 8.86 g of 3-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 11.0 g of N-(3-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.

WORKUP

后处理

  1. customas described in Preparation 1-(3)