HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethoxy(4-phenylbutyl)phosphinyl chloride → HCID 86739549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethoxy(4-phenylbutyl)phosphinyl chloride | HCID 15591238 | — |
| Reactant | HCID 86739550 | HCID 86739550 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86739549 | HCID 86739549 | — |
Reaction Steps
A mixture of crude chloro(4-phenylbutyl)phosphinic acid, ethyl ester, dry methylene chloride and 5-amino-tetrahydro-4-oxo-1,3-thiazepine-3(2H)-acetic acid, ethyl ester are reacted as set forth in Example 1(f). Work up of the reaction mixture according to Example 1(f) yields 5-[[ethoxy(4-phenylbutyl)phosphinyl]amino]tetrahydro-4-oxo-1,3-thiazepine-3(2H)-acetic acid, ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460579 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-7d1c0677baf34c3da179bbb442f969e5 |
| Source note | uspto-grants-1984_07 |