HRID1462488

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID24819

Phosphorus pentachloride

Cl5P

结构：CCOP(=O)(CCCCCCN1C(=O)c2ccccc2C1=O)OCC

HCID256580

2-(6-diethoxyphosphorylhexyl)isoindole-1,3-dione

C18H26NO5P

PRODUCTS

生成物

结构：CCOP(=O)(Cl)CCCCCCN1C(=O)c2ccccc2C1=O

HCID256577

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

A mixture of (6-phthalimidohexyl)phosphonic acid, diethyl ester, benzene, and phosphorus pentachloride is refluxed according to the procedure of Example 1(e) to give chloro(6-phthalimidohexyl) phosphinic acid, ethyl ester.

WORKUP

后处理

temperatureis refluxed