HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → Ethoxy(6-phthalimidohexyl)phosphinyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2-(6-diethoxyphosphorylhexyl)isoindole-1,3-dione | HCID 256580 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Ethoxy(6-phthalimidohexyl)phosphinyl chloride | HCID 256577 | — |
Reaction Steps
A mixture of (6-phthalimidohexyl)phosphonic acid, diethyl ester, benzene, and phosphorus pentachloride is refluxed according to the procedure of Example 1(e) to give chloro(6-phthalimidohexyl) phosphinic acid, ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460579 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-4e1f5296c47040579c022e6103d53556 |
| Source note | uspto-grants-1984_07 |