HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenolate Sodium → HCID 53693383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenolate Sodium | HCID 4445035 | — |
| Reactant | HCID 13089648 | HCID 13089648 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 53693383 | HCID 53693383 | 92% |
Reaction Steps
23.2 g (0.2 mol) of sodium phenolate and 16.5 g (0.1 mol) of 1,1-dichloro-3,3-dimethyl-1,4-pentadiene are heated to 180° C. in 100 ml of N-methylpyrrolidone, during the course of 10 hours. The working-up corresponding to Example A1(a) yields 20.5 g (92% of theory) of 1-chloro-3,3-dimethyl-2-phenoxy-1,4-pentadiene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460793 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-39207f778b9a466097ad78158c62bbf9 |
| Source note | uspto-grants-1984_07 |