HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73678921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| Reactant | HCID 54073519 | HCID 54073519 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 73678921 | HCID 73678921 | 195.2% |
Reaction Steps
The procedure is carried out in the manner described in Example 1(b) but with the use of 122.7 g (0.5 mol) of 3-methyl-12-(3-penten-2-yl)-1-aza-1,5,9-cyclododecatriene, 41.1 g (0.25 mol) of hydroxylamine sulfate, 50 ml of concentrated hydrochloric acid and 250 ml of water. There is obtained on further processing 135.9 g (0.488 mol) of 2-methyl-11-(3-penten-2-yl)-11-amino-undeca-4,8-dienal-oxime; yield 97.6% of theory; nD20 =1.5091.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460790 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-5f15820afa754b8cb4e4c6100fa35e6e |
| Source note | uspto-grants-1984_07 |