Dimethylamine → HCID 13337522, compound

HRID 1462993Notes

Reaction equation

HRID 1462993 reaction equation
[C:1]([C:5]1[CH:24]=[CH:23][CH:22]=[CH:21][C:6]=1[C:7]([NH:9][N:10]([CH3:20])[C:11]([NH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[S:12])=[O:8])([O:3]C)=O.C(OCC)C.[CH3:30][NH:31][CH3:32]>>[CH3:30][N:31]([CH3:32])[C:1]([C:5]1[CH:24]=[CH:23][CH:22]=[CH:21][C:6]=1[C:7]([NH:9][N:10]([CH3:20])[C:11]([NH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[S:12])=[O:8])=[O:3]

Participants

4

Reactant 3

HCID 674DimethylamineHCID 3283Diethyl EtherHCID 13035054HCID 13035054, compound

Product 1

HCID 13337522HCID 13337522, compound

Procedure

1-(2-Carbomethoxybenzoyl)-2-methyl-4-phenyl-3-thiosemicarbazide (5 g, 0.148 mole) was suspended in aqueous dimethylamine. The pH of the suspension was adjusted to about 3. A tacky precipitate was formed which become solid after addition of diethyl ether. This solid--title product--had a melting point of 140°-143°, yield 3.7 g.

Workup

  1. customA tacky precipitate was formed which

Sources & evidence

ORD record
ord-d5bda335f061443d817c5c45812deb37
Source dataset
uspto-grants-1984_07
Patent number
US04462821

Reaction notes

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