HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 13337522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 13035054 | HCID 13035054 | — |
| Product | HCID 13337522 | HCID 13337522 | — |
Reaction Steps
1-(2-Carbomethoxybenzoyl)-2-methyl-4-phenyl-3-thiosemicarbazide (5 g, 0.148 mole) was suspended in aqueous dimethylamine. The pH of the suspension was adjusted to about 3. A tacky precipitate was formed which become solid after addition of diethyl ether. This solid--title product--had a melting point of 140°-143°, yield 3.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04462821 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-d5bda335f061443d817c5c45812deb37 |
| Source note | uspto-grants-1984_07 |