HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Amino-3-nitrophenyl)acetonitrile → HCID 14891906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Amino-3-nitrophenyl)acetonitrile | HCID 14891905 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14891906 | HCID 14891906 | — |
Reaction Steps
A solution of 1-amino-2-nitro-4-cyanomethylbenzene (6 g.) in ethanol (100 ml.) was hydrogenated for 1.5 hour at atmospheric pressure in presence of 3.6 g. of 10% w/w Pd/C. The catalyst was removed and the solvent was evaporated to give 1,2-diamino-4-cyanomethylbenzene which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04463173 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-7c81f0484f1f4f928e631eec9aaac12e |
| Source note | uspto-grants-1984_07 |