関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phosphate | HCID 1061 | — |
| 反応物 | Trisodium Phosphate | HCID 24243 | — |
| 反応物 | Stannous Chloride | HCID 24479 | — |
| 反応物 | Tin atom | HCID 5352426 | — |
| 反応物 | HCID 178527091 | HCID 178527091 | — |
| 反応物 | HCID 178527092 | HCID 178527092 | — |
| 触媒 | Cetylpyridinium chloride monohydrate | HCID 22324 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178527093 | HCID 178527093 | — |
反応手順
The following formulations were tested to determine the substantivity of cetylpyridinium chloride to HAP that had been treated with the test compounds in a separate step, prior to exposing the HAP to the cetylpyridinium chloride; water (control); phytic acid; sodium phosphate (NaH2PO4); and tin/phytic acid/phosphate (Sn-PaP). The phytic acid was used at 0.0015M and prepared from a 0.045M stock solution by removing a 5 mL aliquot to a vial and diluting with 10 mL of water. The pH of this solution was 2.5. The tin/phytic acid solution in 0.5M phosphate buffer was prepared by weighing 0.0051±0.0001 g SnCl2 into a vial and brought into solution by the addition of 5 mL of water. A 5 mL aliquot of 0.0045M phytic acid and a 5 mL aliquot of 1.5M phosphate buffer were added to the tin solution to produce a formulation with 0.0015M Sn; 0.0015M phytic acid; and 0.5M phosphate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05300289 |
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| 出典データセット | uspto-grants-1994_04 |
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| ORD ID | ord-e0cb3e13016148c692076880f645554c |
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| 出典メモ | uspto-grants-1994_04 |
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