反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The following formulations were tested to determine the substantivity of cetylpyridinium chloride to HAP that had been treated with the test compounds in a separate step, prior to exposing the HAP to the cetylpyridinium chloride; water (control); phytic acid; sodium phosphate (NaH2PO4); and tin/phytic acid/phosphate (Sn-PaP). The phytic acid was used at 0.0015M and prepared from a 0.045M stock solution by removing a 5 mL aliquot to a vial and diluting with 10 mL of water. The pH of this solution was 2.5. The tin/phytic acid solution in 0.5M phosphate buffer was prepared by weighing 0.0051±0.0001 g SnCl2 into a vial and brought into solution by the addition of 5 mL of water. A 5 mL aliquot of 0.0045M phytic acid and a 5 mL aliquot of 1.5M phosphate buffer were added to the tin solution to produce a formulation with 0.0015M Sn; 0.0015M phytic acid; and 0.5M phosphate.
WORKUP
后处理
- additionhad been treated with the test compounds in a separate step
- customprepared from a 0.045M stock solution
- customby removing a 5 mL aliquot to a vial and
- additiondiluting with 10 mL of water