Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Peracetic Acid | HCID 6585 | — |
| Reactant | HCID 14282695 | HCID 14282695 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178474343 | HCID 178474343 | — |
Reaction Steps
200 mL 30% peracetic acid in acetic acid was slowly added to a solution of 50 g 4-acetylamino-2,3-dimethylpyridine in 100 mL glacial acetic acid at 60° C. The solution was held at 70° C. for 12 hours then reduced under vacuum heated by a 50° C. water bath. Yield, 58 g N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05300478 |
|---|
| Source dataset | uspto-grants-1994_04 |
|---|
| ORD ID | ord-23033601f347461a9d1eb13bcf908697 |
|---|
| Source note | uspto-grants-1994_04 |
|---|
