反应详情

A solution of 0.5 gram (0.001 mole) of 4,6-diamino-1,2-dihydro 2,2-dimethyl-1-(2,4,5-trichlorophenylmethoxy)-1,3,5-triazine hydrobromide (Compound 60 - Prepared in Example 3) in 30 ml of water was stirred and 1 ml (0.007 mole) of triethylamine was added. The resultant solid was collected by filtration and dried, yielding 0.4 gram of 4,6-diamino-1,2-dihydro-2,2-dimethyl-1-(2,4,5-trichlorophenylmethoxy)-1,3,5-triazine. The NMR spectrum was consistent with the proposed structure.

1. filtrationThe resultant solid was collected by filtration
2. customdried