HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 22851212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Amino-L-phenylalanine methyl ester | HCID 20610830 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22851212 | HCID 22851212 | 100% |
Reaction Steps
To a stirred solution of p-aminophenylalanine methyl ester (1.7 g, 8.8 mmol) in ethanol (150 ml) was added methylamine in ethanol (33%/8M) (100 ml). After stirring at room temperature for 24 hours the reaction mixture was reduced under pressure to yield the title compound as a brown solid (1.7 g, 100%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05300674 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-125e1dae273a4cdd924102ecc637f885 |
| Source note | uspto-grants-1994_04 |