Oxalyl chloride → HCID 53645908, compound

HRID 1463706Notes

Reaction equation

C(Cl)(=O)[C:2](Cl)=[O:3].[NH2:7][C:8]1[N:13]=[C:12]([NH:14][CH2:15][CH2:16][CH2:17][CH2:18][CH:19]2[CH2:24][C:23]([CH3:26])([CH3:25])[N:22]([O:27][CH:28]3[CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]3)[C:21]([CH3:35])([CH3:34])[CH2:20]2)[N:11]=[C:10]([NH:36][CH2:37][CH2:38][CH2:39][CH2:40][CH:41]2[CH2:46][C:45]([CH3:48])([CH3:47])[N:44]([O:49][CH:50]3[CH2:55][CH2:54][CH2:53][CH2:52][CH2:51]3)[C:43]([CH3:57])([CH3:56])[CH2:42]2)[N:9]=1>>[CH:28]1([O:27][N:22]2[C:23]([CH3:25])([CH3:26])[CH2:24][CH:19]([CH2:18][CH2:17][CH2:16][CH2:15][NH:14][C:12]3[N:11]=[C:10]([NH:36][CH2:37][CH2:38][CH2:39][CH2:40][CH:41]4[CH2:42][C:43]([CH3:57])([CH3:56])[N:44]([O:49][CH:50]5[CH2:51][CH2:52][CH2:53][CH2:54][CH2:55]5)[C:45]([CH3:47])([CH3:48])[CH2:46]4)[N:9]=[C:8]([N:7]=[C:2]=[O:3])[N:13]=3)[CH2:20][C:21]2([CH3:34])[CH3:35])[CH2:29][CH2:30][CH2:31][CH2:32][CH2:33]1

Participants

Reactant 2

HCID 65578Oxalyl chloride

HCID 54289188HCID 54289188, compound

Product 1

HCID 53645908HCID 53645908, compound

Procedure

The title compound is prepared from the reaction of oxalyl chloride with the compound prepared in Example 22.

Sources & evidence

ORD record: ord-a47d7a1a19894fefb6df529aa8415824
Source dataset: uspto-grants-1994_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05300544

Reaction notes

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