HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylvaleric acid → 3-Hydroxy-2-methyl-2-propyl-4-phenylmethylenedecanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylvaleric acid | HCID 7341 | — |
| Reactant | 2-(Phenylmethylene)octanal | HCID 7585 | — |
| Product | 3-Hydroxy-2-methyl-2-propyl-4-phenylmethylenedecanoic acid | HCID 54368704 | — |
Reaction Steps
The reaction of 5.8 g (0.05 mole) 2-methylvaleric acid with 10.8 (0.05 mole) of α-hexylcinnamaldehyde was conducted in the manner described in Example III, Method B. The product was isolated as a viscous yellow oil. NMR spectra confirmed the title structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05301693 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-faa08e4ee1064cecbfa95b2ecd2da1eb |
| Source note | uspto-grants-1994_04 |