2-Methylvaleric acid → 3-Hydroxy-2-methyl-2-propyl-4-phenylmethylenedecanoic acid

HRID 1463728Notes

Reaction equation

HRID 1463728 reaction equation
[CH3:1][CH:2]([CH2:6][CH2:7][CH3:8])[C:3]([OH:5])=[O:4].[CH2:9]([C:15](=[CH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH:16]=[O:17])[CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>>[OH:17][CH:16]([C:15](=[CH:18][C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:2]([CH3:1])([CH2:6][CH2:7][CH3:8])[C:3]([OH:5])=[O:4]

Participants

3

Reactant 2

HCID 73412-Methylvaleric acidHCID 75852-(Phenylmethylene)octanal

Product 1

HCID 543687043-Hydroxy-2-methyl-2-propyl-4-phenylmethylenedecanoic acid

Procedure

The reaction of 5.8 g (0.05 mole) 2-methylvaleric acid with 10.8 (0.05 mole) of α-hexylcinnamaldehyde was conducted in the manner described in Example III, Method B. The product was isolated as a viscous yellow oil. NMR spectra confirmed the title structure.

Workup

  1. customThe product was isolated as a viscous yellow oil

Sources & evidence

ORD record
ord-faa08e4ee1064cecbfa95b2ecd2da1eb
Source dataset
uspto-grants-1994_04
Patent number
US05301693

Reaction notes

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