Hydrazine hydrate (1:1) → HCID 86747743, compound

HRID 1463736Notes

Reaction equation

O.[NH2:2][NH2:3].[C:4]([NH:23]N)(=[O:22])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11]/[CH:12]=[CH:13]\[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>>[C:4]([NH2:23])(=[O:22])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11]/[CH:12]=[CH:13]\[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21].[NH2:2][NH2:3]

Participants

Reactant 2

HCID 24654Hydrazine hydrate (1:1)

HCID 5356845oleic hydrazide

Product 1

HCID 86747743HCID 86747743, compound

Conditions

Temperature: 160 °C

Procedure

To 282 g (1.0 mole) of Industrene 105 oleic acid (available from Humko Chemical Division of Witco Corp.) was added 46.0 g (0.92 mole) of hydrazine monohydrate (0.92 moles hydrazine per mole of oleic acid). The mixture was warmed slowly to 160° C. while stripping with nitrogen and stirred for one hour to give 299 g of hydrazine oleamide (or oleic hydrazide). The silver wear and copper corrosion results are reported in Table II below.

Sources & evidence

ORD record: ord-b96b302eb22e49869c7d38d0ab6baed1
Source dataset: uspto-grants-1994_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05302304

Reaction notes

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