Triethylamine → HCID 131718378, compound

Participants

Reaction Steps

4.69 g [59] (24.3 mmol) in 100 ml dichloromethane was carefully added dropwise to a mixture of 6.67 g of 2-methoxybenzyl amine (48.6 mmol) and 5.06 g of triethylamine (50 mmol) in 100 ml diochloromethane, with exclusion of moisture. The mixture was agitated at room temperature for a further three hours, then repeatedly extracted with chloroform after adding water. The organic phase was successively washed with 1N HCl, saturated potassium carbonate solution and water and dried over sodium sulphate.

Provenance & Evidence