HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 3-(1-Methylpiperazin-2-YL)propan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 3-(N-methylpiperazinyl)propylphthalimide | HCID 53787723 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(1-Methylpiperazin-2-YL)propan-1-amine | HCID 45099464 | — |
Reaction Steps
Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 3-(N-methylpiperazinyl)propylphthalimide (229 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302593 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-4c3444155e9d48f29cbdb83b19d8f482 |
| Source note | uspto-grants-1994_04 |