HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 6-(N-methylpiperazinyl)hexylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 6-(N-methylpiperazinyl)hexylphthalimide | HCID 54496633 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 6-(N-methylpiperazinyl)hexylamine | HCID 53764248 | — |
Reaction Steps
Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 6-(N-methylpiperazinyl)hexylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302593 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-da055af6af9e4c54897078cdd4c65a02 |
| Source note | uspto-grants-1994_04 |