HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 2(1H)-Quinolinone, 1-ethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 19088458 | HCID 19088458 | — |
| Reactant | HCID 22413835 | HCID 22413835 | — |
| Solvent | Methyl iodide | HCID 6328 | — |
| Product | 2(1H)-Quinolinone, 1-ethyl- | HCID 104603 | — |
Reaction Steps
The 1,2-dihydro-6-iodo-1-ethylquinolin-2-one used as a starting material was obtained using a similar procedure to that described in the portion of Example 1 which is concerned with the preparation of the starting material 1,2-dihydro-6-iodo-1-methylquinolin-2-one, except that ethyl iodide was used in place in methyl iodide. There were thus obtained in turn 1,2-dihydro-1-ethylquinolin-2-one, m.p. 52°-54° C., and the required starting material as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302594 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-4d77e357587f4bdbadfa3a99ec7db883 |
| Source note | uspto-grants-1994_04 |