HCID 19088483, compound → 2,2-Diphenyl-5-methylaminopentanamide

Participants

Reaction Steps

A mixture of 5-(N-benzyl-N-methylamino)-2,2-diphenylpentanamide (11 g--see Example 1) and 10% palladium-on-carbon (1.1 g) in ethanol (150 ml) was hydrogenated at room temperature and 50 p.s.i. (344.7 kPa) pressure for 87 hours. The mixture was filtered and the filtrate concentrated in vacuo to give an oil. The oil was triturated with ether to give the title compound as a colourless powder, yield 4.5 g.

Provenance & Evidence