HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19088503, compound → HCID 19088472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19088503 | HCID 19088503 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19088472 | HCID 19088472 | — |
Reaction Steps
10% Palladium-on-carbon was added to a solution of 5-(N-benzyl-N-methylamino)-2,2-diphenyl-5-methylhexanamide (0.6 g--see Example 3) in methanol (19 ml) and formic acid (1 ml). The mixture was stirred at room temperature for 16 hours then filtered and the filtrate concentrated in vacuo to give the title compound as a gum, yield 0.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302595 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-35576e9b257341f38d14e42aec801a9c |
| Source note | uspto-grants-1994_04 |