HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 67877349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67877423 | HCID 67877423 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67877349 | HCID 67877349 | — |
Reaction Steps
The acetal (55) (4.180 g) was treated with potassium carbonate (1.18 g) in methanol (100 ml) at room temperature for 2 hours with stirring. The reaction mixture was neutralized with addition of acetic acid, followed by the usual work up to give a crude product. The crude product was chromatographed on a column of silica gel to give the alcohol (56).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302617 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-574341f5874943c384cda29ece089338 |
| Source note | uspto-grants-1994_04 |