Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1463934Generated: November 1, 2026

Acetic Acid → HCID 67877349, compound

https://huagongshe.com/reaction/1463934

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 67877423HCID 67877423—
SolventMethanolHCID 887—
ProductHCID 67877349HCID 67877349—

Reaction Steps

The acetal (55) (4.180 g) was treated with potassium carbonate (1.18 g) in methanol (100 ml) at room temperature for 2 hours with stirring. The reaction mixture was neutralized with addition of acetic acid, followed by the usual work up to give a crude product. The crude product was chromatographed on a column of silica gel to give the alcohol (56).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05302617
Source datasetuspto-grants-1994_04
ORD IDord-574341f5874943c384cda29ece089338
Source noteuspto-grants-1994_04