HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 86747751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 86746996 | HCID 86746996 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86747751 | HCID 86747751 | — |
Reaction Steps
The ether (57) (4.700 g) was reduced in toluene (80 ml) at -78° C. with diisobutylaluminum hydride (1.5-M, 12 ml) to give the lactol (58).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302617 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-400ff5d6789141b7a2b4c95548edbf20 |
| Source note | uspto-grants-1994_04 |