HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 86747753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 86747752 | HCID 86747752 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86747753 | HCID 86747753 | — |
Reaction Steps
The carboxylic acid (59) was treated with diazomethane in ether (150 ml) to give the methyl ester (60). The crude product obtained after the work-up was chromatographed on a column of silica gel (hexane/ethyl acetate =3/2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302617 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-343372d449c543479508cdab6a3ca08d |
| Source note | uspto-grants-1994_04 |