HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 86747755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 86747757 | HCID 86747757 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86747755 | HCID 86747755 | — |
Reaction Steps
The titled compound was prepared substantially in accordance with the method detailed in Example 1 using 2.60 g (5 mmol) of p-nitrobenzyl-3-[(S)-4-phenyloxazolidin-2-one-3-yl]-4-[2-furylethyl]-azetidin-2-one-1-ethanoate, 20 ml of ethyl acetate and 2.0 g (15 mmol) of lithium iodide. The reaction mixture was allowed to react for approximately 71/2 hours at reflux temperature to provide 1.54 g of a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302711 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-fa88b1753fc041f4b568b6c2742aa8ff |
| Source note | uspto-grants-1994_04 |