Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Aminobiphenyl | HCID 7015 | — |
| Reactant | Cyanocyclohexane | HCID 69834 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 178511973 | HCID 178511973 | — |
Reaction Steps
A mixture of 2-aminobiphenyl (3.4 g), cyclohexane carbonitrile (6.5 g) and anhydrous aluminium chloride (8 g) was heated at 100° C. for 8 hours then at 120° C. for 8 hours to yield a product which was purified by chromatography on a neutral alumina column which was eluted with dichloromethane to give N-(2-biphenylyl)-cyclohexane-1-carboxamidine (m.p. 148°-150° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05302720 |
|---|
| Source dataset | uspto-grants-1994_04 |
|---|
| ORD ID | ord-e7fc1b95cebc4a0684120a32b4005fba |
|---|
| Source note | uspto-grants-1994_04 |
|---|
